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Total Synthesis of [Ψ[C(=S)NH]Tpg(4)]Vancomycin Aglycon, [Ψ[C(=NH)NH]Tpg(4)]Vancomycin Aglycon, and Related Key Compounds: Reengineering Vancomycin for Dual d-Ala-d-Ala and d-Ala-d-Lac Binding
The total synthesis of [Ψ[C(=S)NH]Tpg(4)]vancomycin aglycon (8) and its unique AgOAc-promoted single-step conversion to [Ψ[C(=NH)NH]Tpg(4)]vancomycin aglycon (7), conducted on a fully deprotected substrate, are disclosed. The synthetic approach not only permits access to 7, but it also allows late s...
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| Main Authors: | , , , , , , |
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| Formato: | Artigo |
| Idioma: | Inglês |
| Publicado em: |
2012
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| Assuntos: | |
| Acesso em linha: | https://ncbi.nlm.nih.gov/pmc/articles/PMC3262083/ https://ncbi.nlm.nih.gov/pubmed/22188323 https://ncbi.nlm.nih.govhttp://dx.doi.org/10.1021/ja209937s |
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