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Spectroscopic Investigations of [FeFe] Hydrogenase Maturated with [(57)Fe(2)(adt)(CN)(2)(CO)(4)](2–)
The preparation and spectroscopic characterization of a CO-inhibited [FeFe] hydrogenase with a selectively (57)Fe-labeled binuclear subsite is described. The precursor [(57)Fe(2)(adt)(CN)(2)(CO)(4)](2–) was synthesized from the (57)Fe metal, S(8), CO, (NEt(4))CN, NH(4)Cl, and CH(2)O. (Et(4)N)(2)[(57...
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| Udgivet i: | J Am Chem Soc |
|---|---|
| Main Authors: | , , , , , , , , |
| Format: | Artigo |
| Sprog: | Inglês |
| Udgivet: |
2015
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| Fag: | |
| Online adgang: | https://ncbi.nlm.nih.gov/pmc/articles/PMC4799848/ https://ncbi.nlm.nih.gov/pubmed/26091969 https://ncbi.nlm.nih.govhttp://dx.doi.org/10.1021/jacs.5b03270 |
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