Dynamic nuclear polarization-enhanced (1)H–(13)C double resonance NMR in static samples below 20 K

We demonstrate the feasibility of one-dimensional and two-dimensional (1)H–(13)C double resonance NMR experiments with dynamic nuclear polarization (DNP) at 9.4 T and temperatures below 20 K, including both (1)H–(13)C cross-polarization and (1)H decoupling, and discuss the effects of polarizing agen...

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Main Authors: Potapov, Alexey, Thurber, Kent R., Yau, Wai-Ming, Tycko, Robert
Formato: Artigo
Idioma:Inglês
Publicado em: 2012
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Article
Acesso em linha:https://ncbi.nlm.nih.gov/pmc/articles/PMC3727229/
https://ncbi.nlm.nih.gov/pubmed/22743540
https://ncbi.nlm.nih.govhttp://dx.doi.org/10.1016/j.jmr.2012.05.008
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