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Solid state nuclear magnetic resonance with magic-angle spinning and dynamic nuclear polarization below 25 K
We describe an apparatus for solid state nuclear magnetic resonance (NMR) with dynamic nuclear polarization (DNP) and magic-angle spinning (MAS) at 20–25 K and 9.4 Tesla. The MAS NMR probe uses helium to cool the sample space and nitrogen gas for MAS drive and bearings, as described earlier (Thurber...
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| Main Authors: | , , , |
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| Formato: | Artigo |
| Idioma: | Inglês |
| Publicado em: |
2012
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| Assuntos: | |
| Acesso em linha: | https://ncbi.nlm.nih.gov/pmc/articles/PMC3529848/ https://ncbi.nlm.nih.gov/pubmed/23238592 https://ncbi.nlm.nih.govhttp://dx.doi.org/10.1016/j.jmr.2012.11.009 |
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