Solid state nuclear magnetic resonance with magic-angle spinning and dynamic nuclear polarization below 25 K

We describe an apparatus for solid state nuclear magnetic resonance (NMR) with dynamic nuclear polarization (DNP) and magic-angle spinning (MAS) at 20–25 K and 9.4 Tesla. The MAS NMR probe uses helium to cool the sample space and nitrogen gas for MAS drive and bearings, as described earlier (Thurber...

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Main Authors: Thurber, Kent R., Potapov, Alexey, Yau, Wai-Ming, Tycko, Robert
Formato: Artigo
Idioma:Inglês
Publicado: 2012
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Article
Acceso en liña:https://ncbi.nlm.nih.gov/pmc/articles/PMC3529848/
https://ncbi.nlm.nih.gov/pubmed/23238592
https://ncbi.nlm.nih.govhttp://dx.doi.org/10.1016/j.jmr.2012.11.009
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