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Biomolecular solid state NMR with magic-angle spinning at 25 K
A magic-angle spinning (MAS) probe has been constructed which allows the sample to be cooled with helium, while the MAS bearing and drive gases are nitrogen. The sample can be cooled to 25 K using roughly 3 liters/hour of liquid helium, while the 4 mm diameter rotor spins at 6.7 kHz with good stabil...
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| Main Authors: | , |
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| Formato: | Artigo |
| Idioma: | Inglês |
| Publicado em: |
2008
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| Assuntos: | |
| Acesso em linha: | https://ncbi.nlm.nih.gov/pmc/articles/PMC2632798/ https://ncbi.nlm.nih.gov/pubmed/18922715 https://ncbi.nlm.nih.govhttp://dx.doi.org/10.1016/j.jmr.2008.09.015 |
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