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Synthesis and evaluation of nitroxide-based oligoradicals for low-temperature dynamic nuclear polarization in solid state NMR

We describe the synthesis of new nitroxide-based biradical, triradical, and tetraradical compounds and the evaluation of their performance as paramagnetic dopants in dynamic nuclear polarization (DNP) experiments in solid state nuclear magnetic resonance (NMR) spectroscopy with magic-angle spinning...

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Detalhes bibliográficos
Main Authors: Yau, Wai-Ming, Thurber, Kent R., Tycko, Robert
Formato: Artigo
Idioma:Inglês
Publicado em: 2014
Assuntos:
Acesso em linha:https://ncbi.nlm.nih.gov/pmc/articles/PMC4106245/
https://ncbi.nlm.nih.gov/pubmed/24887201
https://ncbi.nlm.nih.govhttp://dx.doi.org/10.1016/j.jmr.2014.05.002
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