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Dynamic nuclear polarization-enhanced (13)C NMR spectroscopy of static biological solids

We explore the possibility of using dynamic nuclear polarization (DNP) to enhance signals in structural studies of biological solids by solid state NMR without sample spinning. Specifically, we use 2D (13)C-(13)C exchange spectroscopy to probe the peptide backbone torsion angles (ϕ,ψ) in a series of...

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Detalhes bibliográficos
Main Authors: Potapov, Alexey, Yau, Wai-Ming, Tycko, Robert
Formato: Artigo
Idioma:Inglês
Publicado em: 2013
Assuntos:
Acesso em linha:https://ncbi.nlm.nih.gov/pmc/articles/PMC3660528/
https://ncbi.nlm.nih.gov/pubmed/23562665
https://ncbi.nlm.nih.govhttp://dx.doi.org/10.1016/j.jmr.2013.02.011
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