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Synthesis of Human Cancer Associated Globo-H (MBr1) Glycosylamino Acid: Some Mechanistic and Conformational Reinvestigations

The synthesis of an extended globo-H (MBr1 antigen) in the form of a glycosylamino acid is reported. By careful NMR analysis, we found an interesting conformational “flip” on the E ring of some synthetic intermediates. An explanation offered for the successful [3+3] coupling of ABC acceptor 11 and D...

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Detalhes bibliográficos
Main Authors: Zhu, Jianglong, Wan, Qian, Yang, Guangbin, Ouerfelli, Ouathek, Danishefsky, Samuel J.
Formato: Artigo
Idioma:Inglês
Publicado em: 2009
Assuntos:
Acesso em linha:https://ncbi.nlm.nih.gov/pmc/articles/PMC3059307/
https://ncbi.nlm.nih.gov/pubmed/21423783
https://ncbi.nlm.nih.govhttp://dx.doi.org/10.3987/COM-08-S(D)82
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