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Synthesis of Cyclic Enones by Allyl-Palladium-Catalyzed α,β-Dehydrogenation
The use of allyl-palladium catalysis for the one-step α,β-dehydrogenation of ketones via their zinc enolates is reported. The optimized protocol utilizes commercially available Zn(TMP)(2) as base and diethyl allyl phosphate as oxidant. Notably, this transformation operates under salt-free conditions...
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| Publicado no: | Org Lett |
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| Main Authors: | , , |
| Formato: | Artigo |
| Idioma: | Inglês |
| Publicado em: |
2018
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| Assuntos: | |
| Acesso em linha: | https://ncbi.nlm.nih.gov/pmc/articles/PMC7913890/ https://ncbi.nlm.nih.gov/pubmed/29327930 https://ncbi.nlm.nih.govhttp://dx.doi.org/10.1021/acs.orglett.7b03818 |
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