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Stereoselective Synthesis of Bicyclo[6.1.0]nonene Precursors of the Bioorthogonal Reagents s-TCO and BCN
The cyclooctyne BCN and the trans-cyclooctene s-TCO are broadly used reagents for bioorthogonal chemistry. A bottleneck for the synthesis of these reagents had been a poorly selective cyclopropanation reaction with ethyl diazoacetate and catalytic Rh(2)(OAc)(4). Here, we describe that low catalyst l...
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| Publicat a: | J Org Chem |
|---|---|
| Autors principals: | , , |
| Format: | Artigo |
| Idioma: | Inglês |
| Publicat: |
2017
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| Matèries: | |
| Accés en línia: | https://ncbi.nlm.nih.gov/pmc/articles/PMC6180907/ https://ncbi.nlm.nih.gov/pubmed/29171257 https://ncbi.nlm.nih.govhttp://dx.doi.org/10.1021/acs.joc.7b02329 |
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