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Stereoselective Synthesis of Bicyclo[6.1.0]nonene Precursors of the Bioorthogonal Reagents s-TCO and BCN
The cyclooctyne BCN and the trans-cyclooctene s-TCO are broadly used reagents for bioorthogonal chemistry. A bottleneck for the synthesis of these reagents had been a poorly selective cyclopropanation reaction with ethyl diazoacetate and catalytic Rh(2)(OAc)(4). Here, we describe that low catalyst l...
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| Yayımlandı: | J Org Chem |
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| Asıl Yazarlar: | , , |
| Materyal Türü: | Artigo |
| Dil: | Inglês |
| Baskı/Yayın Bilgisi: |
2017
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| Konular: | |
| Online Erişim: | https://ncbi.nlm.nih.gov/pmc/articles/PMC6180907/ https://ncbi.nlm.nih.gov/pubmed/29171257 https://ncbi.nlm.nih.govhttp://dx.doi.org/10.1021/acs.joc.7b02329 |
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