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Synthesis of unique spirocyclic orthoester-type derivatives of isothiazolo[4,3-d]pyrimidine nucleosides
A set of unique nucleoside analogs, containing ‘spirocyclic orthoester-type’ scaffolds, were synthesized from a common isothiazolo[4,3-d]pyrimidine-riboside precursor. The key reaction, using 1,2-di-heteroatomic nucleophiles (e.g., 1,2-ethandithiol) and BF(3)•OEt(2), converts an exocyclic imine into...
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| Gepubliceerd in: | J Antibiot (Tokyo) |
|---|---|
| Hoofdauteurs: | , |
| Formaat: | Artigo |
| Taal: | Inglês |
| Gepubliceerd in: |
2017
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| Onderwerpen: | |
| Online toegang: | https://ncbi.nlm.nih.gov/pmc/articles/PMC5785548/ https://ncbi.nlm.nih.gov/pubmed/28743975 https://ncbi.nlm.nih.govhttp://dx.doi.org/10.1038/ja.2017.87 |
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