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Reversible Borylene Formation from Ring Opening of Pinacolborane and Other Intermediates Generated from Five-Coordinate Tris-Boryl Complexes: Implications for Catalytic C–H Borylation
Catalytic C–H borylation using the five-coordinate tris-boryl complex (dippe)Ir(Bpin)(3) (5a, dippe = 1,2-bis(diisopropylphosphino)ethane) has been examined using (31)P{(1)H} and (1)H NMR spectroscopy. Compound 5a was shown to react rapidly and reversibly with HBpin to generate a six-coordinate bory...
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| Udgivet i: | Organometallics |
|---|---|
| Main Authors: | , , , , , , |
| Format: | Artigo |
| Sprog: | Inglês |
| Udgivet: |
2015
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| Fag: | |
| Online adgang: | https://ncbi.nlm.nih.gov/pmc/articles/PMC5297890/ https://ncbi.nlm.nih.gov/pubmed/28190912 https://ncbi.nlm.nih.govhttp://dx.doi.org/10.1021/acs.organomet.5b00525 |
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