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Accurate measurement of (3)J(HNHα) couplings in small or disordered proteins from WATERGATE-optimized TROSY spectra
Provided that care is taken in adjusting the WATERGATE element of a (1)H-(15)N TROSY-HSQC experiment, such that neither the water magnetization nor the (1)H(α) protons are inverted by its final 180° pulse, (3)J(HNHα) couplings can be measured directly from splittings in the (1)H dimension of the spe...
Enregistré dans:
| Publié dans: | J Biomol NMR |
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| Auteurs principaux: | , , |
| Format: | Artigo |
| Langue: | Inglês |
| Publié: |
2015
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| Sujets: | |
| Accès en ligne: | https://ncbi.nlm.nih.gov/pmc/articles/PMC4744140/ https://ncbi.nlm.nih.gov/pubmed/26660434 https://ncbi.nlm.nih.govhttp://dx.doi.org/10.1007/s10858-015-0004-y |
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