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ARTSY-J: Convenient and precise measurement of (3)J(HNH)(α) couplings in medium-size proteins from TROSY-HSQC spectra
A new and convenient method, named ARTSY-J, is introduced that permits extraction of the (3)J(HNHα) couplings in proteins from the relative intensities in a pair of (15)N-(1)H TROSY-HSQC spectra. The pulse scheme includes (3)J(HNHα) dephasing of the narrower TROSY (1)H(N)-{(15)N} doublet component d...
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| Udgivet i: | J Magn Reson |
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| Main Authors: | , , , , |
| Format: | Artigo |
| Sprog: | Inglês |
| Udgivet: |
2016
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| Fag: | |
| Online adgang: | https://ncbi.nlm.nih.gov/pmc/articles/PMC4915346/ https://ncbi.nlm.nih.gov/pubmed/27179455 https://ncbi.nlm.nih.govhttp://dx.doi.org/10.1016/j.jmr.2016.05.001 |
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