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Isolation and Characterisation of Degradation Impurities in the Cefazolin Sodium Drug Substance
Two unknown impurities were detected in the cefazolin sodium bulk drug substance using gradient reversed-phase high-performance liquid chromategraphy (HPLC). These impurities were isolated by preparative HPLC and characterized by using spectroscopic techniques like LC-MS, LC-MS/MS, 1D, 2D NMR, and F...
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| Main Authors: | , , , , , |
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| Formato: | Artigo |
| Idioma: | Inglês |
| Publicado em: |
Österreichische Apotheker-Verlagsgesellschaft
2013
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| Assuntos: | |
| Acesso em linha: | https://ncbi.nlm.nih.gov/pmc/articles/PMC3867249/ https://ncbi.nlm.nih.gov/pubmed/24482765 https://ncbi.nlm.nih.govhttp://dx.doi.org/10.3797/scipharm.1304-14 |
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