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Synthesis and NMR Characterization of (Z,Z,Z,Z,E,E,ω)-Heptaprenol
We describe a practical, multi-gram synthesis of (2Z,6Z,10Z,14Z,18E,22E)-3,7,11,15,19,23,27-heptamethyl-2,6,10,14,18,22,26-octacosaheptaen-1-ol [(Z(4),E(2),ω)-heptaprenol, 4] using the nerol-derived sulfone 8 as the key intermediate. Sulfone 8 is prepared by the literature route, and is converted in...
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| Main Authors: | , , , , |
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| Formato: | Artigo |
| Idioma: | Inglês |
| Publicado em: |
2012
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| Assuntos: | |
| Acesso em linha: | https://ncbi.nlm.nih.gov/pmc/articles/PMC3469273/ https://ncbi.nlm.nih.gov/pubmed/22861066 https://ncbi.nlm.nih.govhttp://dx.doi.org/10.1021/ja306184m |
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