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Discovery of competing anaerobic and aerobic pathways in umpolung amide synthesis allows for site-selective amide (18)O-labeling

The mechanism of umpolung amide synthesis was probed by interrogating potential sources for the oxygen of the product amide carbonyl that emanates from the α-bromo nitroalkane substrate. Using a series of (18)O-labeled substrates and reagents, evidence is gathered to advance two pathways from the pu...

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Hlavní autoři: Shackleford, Jessica P., Shen, Bo, Johnston, Jeffrey N.
Médium: Artigo
Jazyk:Inglês
Vydáno: National Academy of Sciences 2012
Témata:
On-line přístup:https://ncbi.nlm.nih.gov/pmc/articles/PMC3252937/
https://ncbi.nlm.nih.gov/pubmed/22184227
https://ncbi.nlm.nih.govhttp://dx.doi.org/10.1073/pnas.1113553108
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