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HNCA-TOCSY-CANH experiments with alternate (13)C-(12)C labeling: a set of 3D experiment with unique supra-sequential information for mainchain resonance assignment

Described here is a set of three-dimensional (3D) NMR experiments that rely on CACA-TOCSY magnetization transfer via the weak (3)J(C)(α)(C)(α) coupling. These pulse sequences, which resemble recently described (13)C detected CACA-TOCSY (Takeuchi et al. 2010) experiments, are recorded in (1)H(2)O, an...

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Detaylı Bibliyografya
Asıl Yazarlar: Takeuchi, Koh, Gal, Maayan, Takahashi, Hideo, Shimada, Ichio, Wagner, Gerhard
Materyal Türü: Artigo
Dil:Inglês
Baskı/Yayın Bilgisi: 2010
Konular:
Online Erişim:https://ncbi.nlm.nih.gov/pmc/articles/PMC3072286/
https://ncbi.nlm.nih.gov/pubmed/21110064
https://ncbi.nlm.nih.govhttp://dx.doi.org/10.1007/s10858-010-9456-2
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