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CACA-TOCSY with alternate (13)C–(12)C labeling: a (13)C(α) direct detection experiment for mainchain resonance assignment, dihedral angle information, and amino acid type identification

We present a (13)C direct detection CACA-TOCSY experiment for samples with alternate (13)C–(12)C labeling. It provides inter-residue correlations between (13)C(α) resonances of residue i and adjacent C(α)s at positions i − 1 and i + 1. Furthermore, longer mixing times yield correlations to C(α) nucl...

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Detaylı Bibliyografya
Asıl Yazarlar: Takeuchi, Koh, Frueh, Dominique P., Sun, Zhen-Yu J., Hiller, Sebastian, Wagner, Gerhard
Materyal Türü: Artigo
Dil:Inglês
Baskı/Yayın Bilgisi: 2010
Konular:
Online Erişim:https://ncbi.nlm.nih.gov/pmc/articles/PMC2868269/
https://ncbi.nlm.nih.gov/pubmed/20383561
https://ncbi.nlm.nih.govhttp://dx.doi.org/10.1007/s10858-010-9410-3
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