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HNCA-TOCSY-CANH experiments with alternate (13)C-(12)C labeling: a set of 3D experiment with unique supra-sequential information for mainchain resonance assignment
Described here is a set of three-dimensional (3D) NMR experiments that rely on CACA-TOCSY magnetization transfer via the weak (3)J(C)(α)(C)(α) coupling. These pulse sequences, which resemble recently described (13)C detected CACA-TOCSY (Takeuchi et al. 2010) experiments, are recorded in (1)H(2)O, an...
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| Autors principals: | , , , , |
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| Format: | Artigo |
| Idioma: | Inglês |
| Publicat: |
2010
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| Matèries: | |
| Accés en línia: | https://ncbi.nlm.nih.gov/pmc/articles/PMC3072286/ https://ncbi.nlm.nih.gov/pubmed/21110064 https://ncbi.nlm.nih.govhttp://dx.doi.org/10.1007/s10858-010-9456-2 |
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