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A Formal Synthesis of the C1-C9 Fragment of Amphidinolide C Employing the Tamaru Reaction

[Image: see text] Homoallylation of aldehydes with isoprene and triethyl borane, catalyzed by Ni(acac)(2) gave hydroxy alkenes in good yield with excellent regio- and stereoselectivity. Cross metathesis of the hydroxy alkenes with methyl acrylate using second generation Grubbs catalyst and copper(I)...

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Autori principali: Paudyal, Mahesh P., Rath, Nigam P., Spilling, Christopher D.
Natura: Artigo
Lingua:Inglês
Pubblicazione: 2010
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Accesso online:https://ncbi.nlm.nih.gov/pmc/articles/PMC2896498/
https://ncbi.nlm.nih.gov/pubmed/20527780
https://ncbi.nlm.nih.govhttp://dx.doi.org/10.1021/ol100959a
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