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Optimization of the Ugi Reaction Using Parallel Synthesis and Automated Liquid Handling

The optimization of a Ugi reaction involving the mixing of furfurylamine, benzaldehyde, boc-glycine and t-butylisocyanide is described. Triplicate runs of 48 parallel experiments are reported, varying concentration, solvent and the excess of some of the reagents. The isolation of the product was ach...

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Main Authors: Bradley, Jean-Claude, Baig Mirza, Khalid, Osborne, Tom, Wiliams, Antony, Owens, Kevin
Formato: Artigo
Idioma:Inglês
Publicado: MyJove Corporation 2008
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Acceso en liña:https://ncbi.nlm.nih.gov/pmc/articles/PMC2762777/
https://ncbi.nlm.nih.gov/pubmed/19066532
https://ncbi.nlm.nih.govhttp://dx.doi.org/10.3791/942
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