Загрузка...
In Situ Temperature Jump Dynamic Nuclear Polarization: Enhanced Sensitivity in Two Dimensional (13)C-(13)C Correlation Spectroscopy in Solution
Dynamic nuclear polarization is combined with temperature jump methods to develop a new 2D (13)C- (13)C NMR experiment that yields a factor or 100-170 increase insensitivity. The polaization step is performed at ∼100 K and the sample is subsequently melted with a 10.6 mm laser pulse to yield a sampl...
Сохранить в:
| Главные авторы: | , , , |
|---|---|
| Формат: | Artigo |
| Язык: | Inglês |
| Опубликовано: |
2009
|
| Предметы: | |
| Online-ссылка: | https://ncbi.nlm.nih.gov/pmc/articles/PMC2651030/ https://ncbi.nlm.nih.gov/pubmed/18942782 https://ncbi.nlm.nih.govhttp://dx.doi.org/10.1021/ja805521y |
| Метки: |
Добавить метку
Нет меток, Требуется 1-ая метка записи!
|