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In Situ Temperature Jump Dynamic Nuclear Polarization: Enhanced Sensitivity in Two Dimensional (13)C-(13)C Correlation Spectroscopy in Solution
Dynamic nuclear polarization is combined with temperature jump methods to develop a new 2D (13)C- (13)C NMR experiment that yields a factor or 100-170 increase insensitivity. The polaization step is performed at ∼100 K and the sample is subsequently melted with a 10.6 mm laser pulse to yield a sampl...
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| Asıl Yazarlar: | , , , |
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| Materyal Türü: | Artigo |
| Dil: | Inglês |
| Baskı/Yayın Bilgisi: |
2009
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| Konular: | |
| Online Erişim: | https://ncbi.nlm.nih.gov/pmc/articles/PMC2651030/ https://ncbi.nlm.nih.gov/pubmed/18942782 https://ncbi.nlm.nih.govhttp://dx.doi.org/10.1021/ja805521y |
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