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Measurement of sample temperatures under magic-angle spinning from the chemical shift and spin-lattice relaxation rate of (79)Br in KBr powder

Accurate determination of sample temperatures in solid state nuclear magnetic resonance (NMR) with magic-angle spinning (MAS) can be problematic, particularly because frictional heating and heating by radio-frequency irradiation can make the internal sample temperature significantly different from t...

詳細記述

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書誌詳細
主要な著者: Thurber, Kent R., Tycko, Robert
フォーマット: Artigo
言語:Inglês
出版事項: 2008
主題:
オンライン・アクセス:https://ncbi.nlm.nih.gov/pmc/articles/PMC2632797/
https://ncbi.nlm.nih.gov/pubmed/18930418
https://ncbi.nlm.nih.govhttp://dx.doi.org/10.1016/j.jmr.2008.09.019
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