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Measurement of sample temperatures under magic-angle spinning from the chemical shift and spin-lattice relaxation rate of (79)Br in KBr powder
Accurate determination of sample temperatures in solid state nuclear magnetic resonance (NMR) with magic-angle spinning (MAS) can be problematic, particularly because frictional heating and heating by radio-frequency irradiation can make the internal sample temperature significantly different from t...
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| Main Authors: | , |
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| Formato: | Artigo |
| Idioma: | Inglês |
| Publicado em: |
2008
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| Assuntos: | |
| Acesso em linha: | https://ncbi.nlm.nih.gov/pmc/articles/PMC2632797/ https://ncbi.nlm.nih.gov/pubmed/18930418 https://ncbi.nlm.nih.govhttp://dx.doi.org/10.1016/j.jmr.2008.09.019 |
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