A microdroplet-accelerated Biginelli reaction: mechanisms and separation of isomers using IMS-MS

Electrospray ionization (ESI) combined with ion mobility spectrometry (IMS) and mass spectrometry (MS) techniques is used to examine the Biginelli reaction in an ensemble of ions generated from droplets. We find evidence for rapid dihydropyrimidinone formation from condensation of ethyl acetoacetate...

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Detaylı Bibliyografya
Yayımlandı:Chem Sci
Asıl Yazarlar: Sahota, Navneet, AbuSalim, Deyaa I., Wang, Melinda L., Brown, Christopher J., Zhang, Zhicaho, El-Baba, Tarick J., Cook, Silas P., Clemmer, David E.
Materyal Türü: Artigo
Dil:Inglês
Baskı/Yayın Bilgisi: Royal Society of Chemistry 2019
Konular:
Chemistry
Online Erişim:https://ncbi.nlm.nih.gov/pmc/articles/PMC6509997/
https://ncbi.nlm.nih.gov/pubmed/31160956
https://ncbi.nlm.nih.govhttp://dx.doi.org/10.1039/c9sc00704k
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