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A microdroplet-accelerated Biginelli reaction: mechanisms and separation of isomers using IMS-MS
Electrospray ionization (ESI) combined with ion mobility spectrometry (IMS) and mass spectrometry (MS) techniques is used to examine the Biginelli reaction in an ensemble of ions generated from droplets. We find evidence for rapid dihydropyrimidinone formation from condensation of ethyl acetoacetate...
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| 出版年: | Chem Sci |
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| 主要な著者: | , , , , , , , |
| フォーマット: | Artigo |
| 言語: | Inglês |
| 出版事項: |
Royal Society of Chemistry
2019
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| 主題: | |
| オンライン･アクセス: | https://ncbi.nlm.nih.gov/pmc/articles/PMC6509997/ https://ncbi.nlm.nih.gov/pubmed/31160956 https://ncbi.nlm.nih.govhttp://dx.doi.org/10.1039/c9sc00704k |
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