A microdroplet-accelerated Biginelli reaction: mechanisms and separation of isomers using IMS-MS

Electrospray ionization (ESI) combined with ion mobility spectrometry (IMS) and mass spectrometry (MS) techniques is used to examine the Biginelli reaction in an ensemble of ions generated from droplets. We find evidence for rapid dihydropyrimidinone formation from condensation of ethyl acetoacetate...

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Detalles Bibliográficos
Publicado en:Chem Sci
Main Authors: Sahota, Navneet, AbuSalim, Deyaa I., Wang, Melinda L., Brown, Christopher J., Zhang, Zhicaho, El-Baba, Tarick J., Cook, Silas P., Clemmer, David E.
Formato: Artigo
Idioma:Inglês
Publicado: Royal Society of Chemistry 2019
Assuntos:
Chemistry
Acceso en liña:https://ncbi.nlm.nih.gov/pmc/articles/PMC6509997/
https://ncbi.nlm.nih.gov/pubmed/31160956
https://ncbi.nlm.nih.govhttp://dx.doi.org/10.1039/c9sc00704k
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