A microdroplet-accelerated Biginelli reaction: mechanisms and separation of isomers using IMS-MS

Electrospray ionization (ESI) combined with ion mobility spectrometry (IMS) and mass spectrometry (MS) techniques is used to examine the Biginelli reaction in an ensemble of ions generated from droplets. We find evidence for rapid dihydropyrimidinone formation from condensation of ethyl acetoacetate...

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Detalhes bibliográficos
Publicado no:Chem Sci
Main Authors: Sahota, Navneet, AbuSalim, Deyaa I., Wang, Melinda L., Brown, Christopher J., Zhang, Zhicaho, El-Baba, Tarick J., Cook, Silas P., Clemmer, David E.
Formato: Artigo
Idioma:Inglês
Publicado em: Royal Society of Chemistry 2019
Assuntos:
Chemistry
Acesso em linha:https://ncbi.nlm.nih.gov/pmc/articles/PMC6509997/
https://ncbi.nlm.nih.gov/pubmed/31160956
https://ncbi.nlm.nih.govhttp://dx.doi.org/10.1039/c9sc00704k
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