A microdroplet-accelerated Biginelli reaction: mechanisms and separation of isomers using IMS-MS

Electrospray ionization (ESI) combined with ion mobility spectrometry (IMS) and mass spectrometry (MS) techniques is used to examine the Biginelli reaction in an ensemble of ions generated from droplets. We find evidence for rapid dihydropyrimidinone formation from condensation of ethyl acetoacetate...

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Udgivet i:Chem Sci
Main Authors: Sahota, Navneet, AbuSalim, Deyaa I., Wang, Melinda L., Brown, Christopher J., Zhang, Zhicaho, El-Baba, Tarick J., Cook, Silas P., Clemmer, David E.
Format: Artigo
Sprog:Inglês
Udgivet: Royal Society of Chemistry 2019
Fag:
Chemistry
Online adgang:https://ncbi.nlm.nih.gov/pmc/articles/PMC6509997/
https://ncbi.nlm.nih.gov/pubmed/31160956
https://ncbi.nlm.nih.govhttp://dx.doi.org/10.1039/c9sc00704k
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