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Enantioselective phase-transfer catalyzed alkylation of 1-methyl-7-methoxy-2-tetralone: an effective route to dezocine

In order to prepare asymmetrically (R)-(+)-1-(5-bromopentyl)-1-methyl-7-methoxy-2-tetralone (3a), a key intermediate of dezocine, 17 cinchona alkaloid-derived catalysts were prepared and screened for the enantioselective alkylation of 1-methyl-7-methoxy-2-tetralone with 1,5-dibromopentane, and the b...

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Wedi'i Gadw mewn:
Manylion Llyfryddiaeth
Cyhoeddwyd yn:Beilstein J Org Chem
Prif Awduron: Li, Ruipeng, Liu, Zhenren, Chen, Liang, Pan, Jing, Zhou, Weicheng
Fformat: Artigo
Iaith:Inglês
Cyhoeddwyd: Beilstein-Institut 2018
Pynciau:
Mynediad Ar-lein:https://ncbi.nlm.nih.gov/pmc/articles/PMC6009193/
https://ncbi.nlm.nih.gov/pubmed/29977405
https://ncbi.nlm.nih.govhttp://dx.doi.org/10.3762/bjoc.14.119
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