High yielding synthesis of 2,2′-bipyridine macrocycles, versatile intermediates in the synthesis of rotaxanes

We present an operationally simple approach to 2,2′-bipyridine macrocycles. Our method uses simple starting materials to produce these previously hard to access rotaxane precursors in remarkable yields (typically >65%) across a range of scales (0.1–5 mmol). All of the macrocycles reported are eff...

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Udgivet i:Chem Sci
Main Authors: Lewis, J. E. M., Bordoli, R. J., Denis, M., Fletcher, C. J., Galli, M., Neal, E. A., Rochette, E. M., Goldup, S. M.
Format: Artigo
Sprog:Inglês
Udgivet: Royal Society of Chemistry 2016
Fag:
Chemistry
Online adgang:https://ncbi.nlm.nih.gov/pmc/articles/PMC6005271/
https://ncbi.nlm.nih.gov/pubmed/29997807
https://ncbi.nlm.nih.govhttp://dx.doi.org/10.1039/c6sc00011h
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