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Competitive formation of homocircuit [3]rotaxanes in synthetically useful yields in the bipyridine-mediated active template CuAAC reaction

We recently identified competitive formation of doubly interlocked [3]rotaxanes as the origin of the non-linear variation in yield of [2]rotaxane with macrocycle size in the bipyridine-mediated AT-CuAAC reaction. Selection of reaction conditions gave [2]rotaxanes in essentially quantitative yield in...

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Detalhes bibliográficos
Publicado no:Chem Sci
Main Authors: Neal, Edward A., Goldup, Stephen M.
Formato: Artigo
Idioma:Inglês
Publicado em: Royal Society of Chemistry 2015
Assuntos:
Acesso em linha:https://ncbi.nlm.nih.gov/pmc/articles/PMC5645920/
https://ncbi.nlm.nih.gov/pubmed/29308153
https://ncbi.nlm.nih.govhttp://dx.doi.org/10.1039/c4sc03999h
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