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Rational design of dinitroxide biradicals for efficient cross-effect dynamic nuclear polarization
A series of 37 dinitroxide biradicals have been prepared and their performance studied as polarizing agents in cross-effect DNP NMR experiments at 9.4 T and 100 K in 1,1,2,2-tetrachloroethane (TCE). We observe that in this regime the DNP performance is strongly correlated with the substituents on th...
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| Publicado en: | Chem Sci |
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| Main Authors: | , , , , , , , , , , , , , |
| Formato: | Artigo |
| Idioma: | Inglês |
| Publicado: |
Royal Society of Chemistry
2016
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| Assuntos: | |
| Acceso en liña: | https://ncbi.nlm.nih.gov/pmc/articles/PMC5952883/ https://ncbi.nlm.nih.gov/pubmed/29896347 https://ncbi.nlm.nih.govhttp://dx.doi.org/10.1039/c5sc02921j |
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