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Site-selective bromination of sp(3) C–H bonds

A method for converting sp(3) C–H to C–Br bonds using an N-methyl sulfamate directing group is described. The reaction employs Rh(2)(oct)(4) and a mixture of NaBr and NaOCl and is performed in aqueous solution open to air. For all sulfamates examined, oxidation occurs with high selectivity at the γ-...

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Bibliografiske detaljer
Udgivet i:Chem Sci
Main Authors: Sathyamoorthi, Shyam, Banerjee, Shibdas, Du Bois, J., Burns, Noah Z., Zare, Richard N.
Format: Artigo
Sprog:Inglês
Udgivet: Royal Society of Chemistry 2017
Fag:
Online adgang:https://ncbi.nlm.nih.gov/pmc/articles/PMC5873043/
https://ncbi.nlm.nih.gov/pubmed/29629078
https://ncbi.nlm.nih.govhttp://dx.doi.org/10.1039/c7sc04611a
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