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O-Acetyl Side-Chains in Monosaccharides: Redundant NMR Spin-Couplings and Statistical Models for Acetate Ester Conformational Analysis
α- and β-D-glucopyranose monoacetates 1–3 were prepared with selective (13)C enrichment in the O-acetyl side-chain, and ensembles of (13)C–(1)H and (13)C–(13)C NMR spin-couplings (J-couplings) were measured involving the labeled carbons. Density functional theory (DFT) was applied to a set of model...
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| Publicado no: | J Phys Chem B |
|---|---|
| Main Authors: | , , , , , , , |
| Formato: | Artigo |
| Idioma: | Inglês |
| Publicado em: |
2016
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| Assuntos: | |
| Acesso em linha: | https://ncbi.nlm.nih.gov/pmc/articles/PMC5556682/ https://ncbi.nlm.nih.gov/pubmed/28001427 https://ncbi.nlm.nih.govhttp://dx.doi.org/10.1021/acs.jpcb.6b10028 |
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