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Conformational Populations of β-(1→4) O-Glycosidic Linkages Using Redundant NMR J-Couplings and Circular Statistics

Twelve disaccharides containing β-(1→4) linkages and displaying systematic structural variations in the vicinity of these linkages were selectively labeled with (13)C to facilitate measurements of multiple NMR spin–spin (scalar; J) coupling constants (J(CH) and J(CC) values) across their O-glycosidi...

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Detalhes bibliográficos
Publicado no:J Phys Chem B
Main Authors: Zhang, Wenhui, Turney, Toby, Meredith, Reagan, Pan, Qingfeng, Sernau, Luke, Wang, Xiaocong, Hu, Xiaosong, Woods, Robert J., Carmichael, Ian, Serianni, Anthony S.
Formato: Artigo
Idioma:Inglês
Publicado em: 2017
Assuntos:
Acesso em linha:https://ncbi.nlm.nih.gov/pmc/articles/PMC5553453/
https://ncbi.nlm.nih.gov/pubmed/28296420
https://ncbi.nlm.nih.govhttp://dx.doi.org/10.1021/acs.jpcb.7b02252
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