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Effect of uridine protecting groups on the diastereoselectivity of uridine-derived aldehyde 5’-alkynylation

The 5’-alkynylation of uridine-derived aldehydes is described. The addition of alkynyl Grignard reagents on the carbonyl group is significantly influenced by the 2’,3’-di-O-protecting groups (R(1)): O-alkyl groups led to modest diastereoselectivities (65:35) in favor of the 5’R-isomer, whereas O-sil...

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Detalhes bibliográficos
Publicado no:Beilstein J Org Chem
Main Authors: Ben Othman, Raja, Fer, Mickaël J, Le Corre, Laurent, Calvet-Vitale, Sandrine, Gravier-Pelletier, Christine
Formato: Artigo
Idioma:Inglês
Publicado em: Beilstein-Institut 2017
Assuntos:
Acesso em linha:https://ncbi.nlm.nih.gov/pmc/articles/PMC5550804/
https://ncbi.nlm.nih.gov/pubmed/28845198
https://ncbi.nlm.nih.govhttp://dx.doi.org/10.3762/bjoc.13.153
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