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Multigram-scale Synthesis of Enantiopure 3,3-Difluoroproline
An efficient route for the synthesis of enantiopure 3,3-difluoroproline on multigram-scale is described herein. The deoxofluorination can be achieved with DAST on the corresponding racemic pyrrolidinone in good yield. Resolution of the racemate by crystallization with D- and L-tyrosine hydrazide pro...
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| Publicado no: | Tetrahedron Lett |
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| Main Authors: | , , |
| Formato: | Artigo |
| Idioma: | Inglês |
| Publicado em: |
2016
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| Assuntos: | |
| Acesso em linha: | https://ncbi.nlm.nih.gov/pmc/articles/PMC5456297/ https://ncbi.nlm.nih.gov/pubmed/28584384 https://ncbi.nlm.nih.govhttp://dx.doi.org/10.1016/j.tetlet.2016.11.012 |
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