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Ruthenium-BINAP Catalyzed Alcohol C-H tert-Prenylation via 1,3-Enyne Transfer Hydrogenation: Beyond Stoichiometric Carbanions in Enantioselective Carbonyl Propargylation

The chiral ruthenium complex formed in situ from (TFA)(2)Ru(CO)(PPh(3))(2) and (R)-BINAP is found to catalyze the enantioselective C-C coupling of diverse primary alcohols with the 1,3-enyne, TMSC≡CC(Me)=CH(2), to form secondary homopropargyl alcohols bearing gem-dimethyl groups. All reagents for th...

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Publicat a:J Am Chem Soc
Autors principals: Nguyen, Khoa D., Herkommer, Daniel, Krische, Michael J.
Format: Artigo
Idioma:Inglês
Publicat: 2016
Matèries:
Accés en línia:https://ncbi.nlm.nih.gov/pmc/articles/PMC4920142/
https://ncbi.nlm.nih.gov/pubmed/27079149
https://ncbi.nlm.nih.govhttp://dx.doi.org/10.1021/jacs.6b02279
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