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Site-Specific Internal Motions in GB1 Protein Microcrystals Revealed by 3D (2)H–(13)C–(13)C Solid-State NMR Spectroscopy

[Image: see text] (2)H quadrupolar line shapes deliver rich information about protein dynamics. A newly designed 3D (2)H–(13)C–(13)C solid-state NMR magic angle spinning (MAS) experiment is presented and demonstrated on the microcrystalline β1 immunoglobulin binding domain of protein G (GB1). The im...

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Bibliografiska uppgifter
I publikationen:J Am Chem Soc
Huvudupphovsmän: Shi, Xiangyan, Rienstra, Chad M.
Materialtyp: Artigo
Språk:Inglês
Publicerad: American Chemical Society 2016
Länkar:https://ncbi.nlm.nih.gov/pmc/articles/PMC4819898/
https://ncbi.nlm.nih.gov/pubmed/26849428
https://ncbi.nlm.nih.govhttp://dx.doi.org/10.1021/jacs.5b12974
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