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Site-Specific Internal Motions in GB1 Protein Microcrystals Revealed by 3D (2)H–(13)C–(13)C Solid-State NMR Spectroscopy
[Image: see text] (2)H quadrupolar line shapes deliver rich information about protein dynamics. A newly designed 3D (2)H–(13)C–(13)C solid-state NMR magic angle spinning (MAS) experiment is presented and demonstrated on the microcrystalline β1 immunoglobulin binding domain of protein G (GB1). The im...
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| Udgivet i: | J Am Chem Soc |
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| Main Authors: | , |
| Format: | Artigo |
| Sprog: | Inglês |
| Udgivet: |
American Chemical
Society
2016
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| Online adgang: | https://ncbi.nlm.nih.gov/pmc/articles/PMC4819898/ https://ncbi.nlm.nih.gov/pubmed/26849428 https://ncbi.nlm.nih.govhttp://dx.doi.org/10.1021/jacs.5b12974 |
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