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Short and Efficient Syntheses of Protoberberine Alkaloids using Palladium-Catalyzed Enolate Arylation**

A concise synthesis of the biologically active alkaloid berberine is reported, and a versatile palladium-catalyzed enolate arylation is used to form the isoquinoline core. The overall yield of 50 % is a large improvement over the single, previous synthesis. By design, this modular route allows the r...

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Vydáno v:Angew Chem Int Ed Engl
Hlavní autoři: Gatland, Alice E, Pilgrim, Ben S, Procopiou, Panayiotis A, Donohoe, Timothy J
Médium: Artigo
Jazyk:Inglês
Vydáno: WILEY-VCH Verlag 2014
Témata:
On-line přístup:https://ncbi.nlm.nih.gov/pmc/articles/PMC4502971/
https://ncbi.nlm.nih.gov/pubmed/25348493
https://ncbi.nlm.nih.govhttp://dx.doi.org/10.1002/anie.201409164
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