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Coupling of Sterically Hindered Trisubstituted Olefins and Benzocyclobutenones via C–C Activation: Total Synthesis and Structural Revision of Cycloinumakiol
The first total synthesis of the proposed structure of cycloinumakiol (1) and its C5-epimer (18) are achieved in a concise and efficient fashion: 9 and 5 steps from known 3-hydroxybenzocyclobutenone with overall yields of 15% and 33%, respectively. A key for the success of this approach is use of a...
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| Main Authors: | , |
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| Formato: | Artigo |
| Idioma: | Inglês |
| Publicado em: |
2014
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| Assuntos: | |
| Acesso em linha: | https://ncbi.nlm.nih.gov/pmc/articles/PMC4214140/ https://ncbi.nlm.nih.gov/pubmed/25138969 https://ncbi.nlm.nih.govhttp://dx.doi.org/10.1002/anie.201404802 |
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