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Dithiolopyranthione Synthesis, Spectroscopy and an Unusual Reactivity with DDQ
The bicyclic pyran thiolone tetrahydro-3αH-[1,3]dithiolo[4,5-β]pyran-2-thione (3a) engages in a highly unusual fragmentation in the presence of DDQ. The pyran thiolone, 3a, was synthesized by chlorination of 3,4-dihydro-2H-pyran (1), followed by condensing with CS(2) and NaSH. Reaction of 3a with DD...
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| Main Authors: | , , , , , , |
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| Formato: | Artigo |
| Idioma: | Inglês |
| Publicado em: |
2013
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| Assuntos: | |
| Acesso em linha: | https://ncbi.nlm.nih.gov/pmc/articles/PMC4200397/ https://ncbi.nlm.nih.gov/pubmed/25328243 https://ncbi.nlm.nih.govhttp://dx.doi.org/10.1002/jhet.1715 |
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