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Perturbation of nuclear spin polarizations in solid state NMR of nitroxide-doped samples by magic-angle spinning without microwaves

We report solid state (13)C and (1)H nuclear magnetic resonance (NMR) experiments with magic-angle spinning (MAS) on frozen solutions containing nitroxide-based paramagnetic dopants that indicate significant perturbations of nuclear spin polarizations without microwave irradiation. At temperatures n...

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Main Authors: Thurber, Kent R., Tycko, Robert
格式: Artigo
語言:Inglês
出版: U.S. Government 2014
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在線閱讀:https://ncbi.nlm.nih.gov/pmc/articles/PMC4032438/
https://ncbi.nlm.nih.gov/pubmed/24832263
https://ncbi.nlm.nih.govhttp://dx.doi.org/10.1063/1.4874341
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