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Towards the Total Synthesis of Marineosin A: Construction of the Macrocyclic Pyrrole and an Advanced, Functionalized Spiroaminal Model

Herein, we describe the enantioselective construction of the 12-membered macrocyclic pyrrole core 4 of marineosin A in 5.1% overall yield from (S)-propylene oxide. The route features a key Stetter reaction to install a 1,4-diketone, which is then subjected to Paal-Knorr pyrrole synthesis and ring cl...

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Bibliografische gegevens
Hoofdauteurs: Aldrich, Leslie N., Berry, Cynthia B., Bates, Brittney S., Konkol, Leah C., So, Miranda, Lindsley, Craig W.
Formaat: Artigo
Taal:Inglês
Gepubliceerd in: 2013
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Online toegang:https://ncbi.nlm.nih.gov/pmc/articles/PMC3885260/
https://ncbi.nlm.nih.gov/pubmed/24415906
https://ncbi.nlm.nih.govhttp://dx.doi.org/10.1002/ejoc.201300643
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