A construction of 4,4-spirocyclic γ-lactams by tandem radical cyclization with carbon monoxide

A straightforward synthesis of 4,4-spirocyclic indol γ-lactams by tandem radical cyclization of iodoaryl allyl azides with CO was achieved. The reaction of iodoaryl allyl azides, TTMSS and AIBN under CO pressure (80 atm) in THF at 80 °C gave the desired 4,4-spirocyclic indoline, benzofuran, and oxin...

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Detalhes bibliográficos
Main Authors: Ueda, Mitsuhiro, Uenoyama, Yoshitaka, Terasoma, Nozomi, Doi, Shoko, Kobayashi, Shoji, Ryu, Ilhyong, Murphy, John A
Formato: Artigo
Idioma:Inglês
Publicado em: Beilstein-Institut 2013
Assuntos:
Letter
Acesso em linha:https://ncbi.nlm.nih.gov/pmc/articles/PMC3740707/
https://ncbi.nlm.nih.gov/pubmed/23946829
https://ncbi.nlm.nih.govhttp://dx.doi.org/10.3762/bjoc.9.151
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