HiFSA Fingerprinting Applied to Isomers with Near-Identical NMR Spectra: The Silybin/Isosilybin Case

This study demonstrates how regio- and diastereo-isomers with near-identical NMR spectra can be distinguished and unambiguously assigned using quantum mechanical driven, (1)H iterative Full Spin Analysis (HiFSA). The method is illustrated with four natural products, the flavonolignans silybin A, sil...

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主要な著者: Napolitano, José G., Lankin, David C., Graf, Tyler N., Friesen, J. Brent, Chen, Shao-Nong, McAlpine, James B., Oberlies, Nicholas H., Pauli, Guido F.
フォーマット: Artigo
言語:Inglês
出版事項: 2013
主題:
Article
オンライン･アクセス:https://ncbi.nlm.nih.gov/pmc/articles/PMC3640553/
https://ncbi.nlm.nih.gov/pubmed/23461697
https://ncbi.nlm.nih.govhttp://dx.doi.org/10.1021/jo302720h
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