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The efficiency of DPPH as a polarising agent for DNP-NMR spectroscopy
The free radical 2,2-diphenyl-1-pycrylhydrazyl (DPPH) was tested as a polarising agent for fast dissolution dynamic nuclear polarisation (DNP) NMR spectroscopy. DPPH was found to be reasonably soluble in sulfolane and the optimum concentration for DNP is 20–40 mM depending upon whether short polaris...
Αποθηκεύτηκε σε:
| Κύριοι συγγραφείς: | , , , , , , , |
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| Μορφή: | Artigo |
| Γλώσσα: | Inglês |
| Έκδοση: |
2012
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| Θέματα: | |
| Διαθέσιμο Online: | https://ncbi.nlm.nih.gov/pmc/articles/PMC3507463/ https://ncbi.nlm.nih.gov/pubmed/23205273 https://ncbi.nlm.nih.govhttp://dx.doi.org/10.1039/C2RA21853D |
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